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Bruker: Collecting Data

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Sample Preparation Subtopics

Introduction to Collecting Bruker Data

September 09, 2020 03:41 PM
basic outline of procedure – chemistry computer account – Topspin automation – choosing sample position – sample holder – depth gauge – sample positioning (including Shigemi tubes)

TopSpin Automation Queue

September 09, 2020 03:41 PM
setup study (name, exp #, solvent, chose spectra) – adjusting parameters – day queue vs night queue

Misc Topics

September 09, 2020 03:41 PM
estimating the concentration from a 1H spectrum (i.e., using Eretic) – continuing a previous study – ,isc topics: how to turn off NOE for 13C, coupled HSQC, coupled vs decoupled 31P – estimating signal averaging time based on concentration (examples)

Bruker: Selective 1D & 2D Protocols

September 28, 2020 09:49 PM
1D-selective TOCSY and NOESY – band-selective HSQC and HMBC – running scout spectra – setting up selective protocols under automation – processing data

Bruker: noD-HQ

July 28, 2021 02:35 PM
How to calculate the concentration of a solute in a protonated solvent